Characterization of white poplar and eucalyptus after ionic liquid pretreatment as a function of biomass loading using X-ray diffraction and small angle neutron scattering.
Identifieur interne : 001482 ( Main/Exploration ); précédent : 001481; suivant : 001483Characterization of white poplar and eucalyptus after ionic liquid pretreatment as a function of biomass loading using X-ray diffraction and small angle neutron scattering.
Auteurs : Xueming Yuan [République populaire de Chine] ; Yonghao Duan [République populaire de Chine] ; Lilin He [États-Unis] ; Seema Singh [États-Unis] ; Blake Simmons [États-Unis] ; Gang Cheng [États-Unis]Source :
- Bioresource technology [ 1873-2976 ] ; 2017.
Descripteurs français
- KwdFr :
- Biomasse (MeSH), Cellulose (composition chimique), Diffraction de neutrons (MeSH), Diffraction des rayons X (MeSH), Diffusion aux petits angles (MeSH), Eucalyptus (composition chimique), Hydrolyse (MeSH), Imidazoles (composition chimique), Liquides ioniques (composition chimique), Populus (composition chimique).
- MESH :
- composition chimique : Cellulose, Eucalyptus, Imidazoles, Liquides ioniques, Populus.
- Biomasse, Diffraction de neutrons, Diffraction des rayons X, Diffusion aux petits angles, Hydrolyse.
English descriptors
- KwdEn :
- MESH :
- chemical , chemistry : Cellulose, Imidazoles, Ionic Liquids.
- chemistry : Eucalyptus, Populus.
- Biomass, Hydrolysis, Neutron Diffraction, Scattering, Small Angle, X-Ray Diffraction.
Abstract
A systematic study was performed to understand interactions among biomass loading during ionic liquid (IL) pretreatment, biomass type and biomass structures. White poplar and eucalyptus samples were pretreated using 1-ethyl-3-methylimidazolium acetate (EmimOAc) at 110°C for 3h at biomass loadings of 5, 10, 15, 20 and 25wt%. All of the samples were chemically characterized and tested for enzymatic hydrolysis. Physical structures including biomass crystallinity and porosity were measured by X-ray diffraction (XRD) and small angle neutron scattering (SANS), respectively. SANS detected pores of radii ranging from ∼25 to 625Å, enabling assessment of contributions of pores with different sizes to increased porosity after pretreatment. Contrasting dependences of sugar conversion on white poplar and eucalyptus as a function of biomass loading were observed and cellulose crystalline structure was found to play an important role.
DOI: 10.1016/j.biortech.2017.02.014
PubMed: 28214697
Affiliations:
Links toward previous steps (curation, corpus...)
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Electronic address: gchengbuct@gmail.com.</nlm:affiliation><country xml:lang="fr">États-Unis</country><wicri:regionArea>College of Life Science and Technology, Beijing University of Chemical Technology, Beijing 100029, China; Deconstruction Division, Joint BioEnergy Institute (JBEI), Emeryville, CA 94608, USA; Biological Systems and Engineering Division, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, Berkeley, CA 94720</wicri:regionArea><placeName><region type="state">Californie</region></placeName></affiliation></author></analytic><series><title level="j">Bioresource technology</title><idno type="eISSN">1873-2976</idno><imprint><date when="2017" type="published">2017</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Biomass (MeSH)</term><term>Cellulose (chemistry)</term><term>Eucalyptus (chemistry)</term><term>Hydrolysis (MeSH)</term><term>Imidazoles (chemistry)</term><term>Ionic Liquids (chemistry)</term><term>Neutron Diffraction (MeSH)</term><term>Populus (chemistry)</term><term>Scattering, Small Angle (MeSH)</term><term>X-Ray Diffraction (MeSH)</term></keywords><keywords scheme="KwdFr" xml:lang="fr"><term>Biomasse (MeSH)</term><term>Cellulose (composition chimique)</term><term>Diffraction de neutrons (MeSH)</term><term>Diffraction des rayons X (MeSH)</term><term>Diffusion aux petits angles (MeSH)</term><term>Eucalyptus (composition chimique)</term><term>Hydrolyse (MeSH)</term><term>Imidazoles (composition chimique)</term><term>Liquides ioniques (composition chimique)</term><term>Populus (composition chimique)</term></keywords><keywords scheme="MESH" type="chemical" qualifier="chemistry" xml:lang="en"><term>Cellulose</term><term>Imidazoles</term><term>Ionic Liquids</term></keywords><keywords scheme="MESH" qualifier="chemistry" xml:lang="en"><term>Eucalyptus</term><term>Populus</term></keywords><keywords scheme="MESH" qualifier="composition chimique" xml:lang="fr"><term>Cellulose</term><term>Eucalyptus</term><term>Imidazoles</term><term>Liquides ioniques</term><term>Populus</term></keywords><keywords scheme="MESH" xml:lang="en"><term>Biomass</term><term>Hydrolysis</term><term>Neutron Diffraction</term><term>Scattering, Small Angle</term><term>X-Ray Diffraction</term></keywords><keywords scheme="MESH" xml:lang="fr"><term>Biomasse</term><term>Diffraction de neutrons</term><term>Diffraction des rayons X</term><term>Diffusion aux petits angles</term><term>Hydrolyse</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">A systematic study was performed to understand interactions among biomass loading during ionic liquid (IL) pretreatment, biomass type and biomass structures. White poplar and eucalyptus samples were pretreated using 1-ethyl-3-methylimidazolium acetate (EmimOAc) at 110°C for 3h at biomass loadings of 5, 10, 15, 20 and 25wt%. All of the samples were chemically characterized and tested for enzymatic hydrolysis. Physical structures including biomass crystallinity and porosity were measured by X-ray diffraction (XRD) and small angle neutron scattering (SANS), respectively. SANS detected pores of radii ranging from ∼25 to 625Å, enabling assessment of contributions of pores with different sizes to increased porosity after pretreatment. Contrasting dependences of sugar conversion on white poplar and eucalyptus as a function of biomass loading were observed and cellulose crystalline structure was found to play an important role.</div></front></TEI><pubmed><MedlineCitation Status="MEDLINE" IndexingMethod="Curated" Owner="NLM"><PMID Version="1">28214697</PMID><DateCompleted><Year>2017</Year><Month>05</Month><Day>08</Day></DateCompleted><DateRevised><Year>2018</Year><Month>12</Month><Day>02</Day></DateRevised><Article PubModel="Print-Electronic"><Journal><ISSN IssnType="Electronic">1873-2976</ISSN><JournalIssue CitedMedium="Internet"><Volume>232</Volume><PubDate><Year>2017</Year><Month>May</Month></PubDate></JournalIssue><Title>Bioresource technology</Title><ISOAbbreviation>Bioresour Technol</ISOAbbreviation></Journal><ArticleTitle>Characterization of white poplar and eucalyptus after ionic liquid pretreatment as a function of biomass loading using X-ray diffraction and small angle neutron scattering.</ArticleTitle><Pagination><MedlinePgn>113-118</MedlinePgn></Pagination><ELocationID EIdType="pii" ValidYN="Y">S0960-8524(17)30121-9</ELocationID><ELocationID EIdType="doi" ValidYN="Y">10.1016/j.biortech.2017.02.014</ELocationID><Abstract><AbstractText>A systematic study was performed to understand interactions among biomass loading during ionic liquid (IL) pretreatment, biomass type and biomass structures. White poplar and eucalyptus samples were pretreated using 1-ethyl-3-methylimidazolium acetate (EmimOAc) at 110°C for 3h at biomass loadings of 5, 10, 15, 20 and 25wt%. All of the samples were chemically characterized and tested for enzymatic hydrolysis. Physical structures including biomass crystallinity and porosity were measured by X-ray diffraction (XRD) and small angle neutron scattering (SANS), respectively. SANS detected pores of radii ranging from ∼25 to 625Å, enabling assessment of contributions of pores with different sizes to increased porosity after pretreatment. Contrasting dependences of sugar conversion on white poplar and eucalyptus as a function of biomass loading were observed and cellulose crystalline structure was found to play an important role.</AbstractText><CopyrightInformation>Copyright © 2017 Elsevier Ltd. All rights reserved.</CopyrightInformation></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Yuan</LastName><ForeName>Xueming</ForeName><Initials>X</Initials><AffiliationInfo><Affiliation>College of Life Science and Technology, Beijing University of Chemical Technology, Beijing 100029, China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Duan</LastName><ForeName>Yonghao</ForeName><Initials>Y</Initials><AffiliationInfo><Affiliation>College of Life Science and Technology, Beijing University of Chemical Technology, Beijing 100029, China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>He</LastName><ForeName>Lilin</ForeName><Initials>L</Initials><AffiliationInfo><Affiliation>Biology and Soft Matter Division, Oak Ridge National Laboratory, TN 37830, USA.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Singh</LastName><ForeName>Seema</ForeName><Initials>S</Initials><AffiliationInfo><Affiliation>Deconstruction Division, Joint BioEnergy Institute (JBEI), Emeryville, CA 94608, USA; Sandia National Laboratories, Livermore, CA 94551, USA.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Simmons</LastName><ForeName>Blake</ForeName><Initials>B</Initials><AffiliationInfo><Affiliation>Deconstruction Division, Joint BioEnergy Institute (JBEI), Emeryville, CA 94608, USA; Biological Systems and Engineering Division, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, Berkeley, CA 94720, USA.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Cheng</LastName><ForeName>Gang</ForeName><Initials>G</Initials><AffiliationInfo><Affiliation>College of Life Science and Technology, Beijing University of Chemical Technology, Beijing 100029, China; Deconstruction Division, Joint BioEnergy Institute (JBEI), Emeryville, CA 94608, USA; Biological Systems and Engineering Division, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, Berkeley, CA 94720, USA. Electronic address: gchengbuct@gmail.com.</Affiliation></AffiliationInfo></Author></AuthorList><Language>eng</Language><PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2017</Year><Month>02</Month><Day>08</Day></ArticleDate></Article><MedlineJournalInfo><Country>England</Country><MedlineTA>Bioresour Technol</MedlineTA><NlmUniqueID>9889523</NlmUniqueID><ISSNLinking>0960-8524</ISSNLinking></MedlineJournalInfo><ChemicalList><Chemical><RegistryNumber>0</RegistryNumber><NameOfSubstance UI="D007093">Imidazoles</NameOfSubstance></Chemical><Chemical><RegistryNumber>0</RegistryNumber><NameOfSubstance UI="D052578">Ionic Liquids</NameOfSubstance></Chemical><Chemical><RegistryNumber>9004-34-6</RegistryNumber><NameOfSubstance UI="D002482">Cellulose</NameOfSubstance></Chemical><Chemical><RegistryNumber>TVE1D62MAK</RegistryNumber><NameOfSubstance UI="C518739">1-ethyl-3-methylimidazolium</NameOfSubstance></Chemical></ChemicalList><CitationSubset>IM</CitationSubset><MeshHeadingList><MeshHeading><DescriptorName UI="D018533" MajorTopicYN="Y">Biomass</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D002482" MajorTopicYN="N">Cellulose</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="N">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D005052" MajorTopicYN="N">Eucalyptus</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="Y">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D006868" MajorTopicYN="N">Hydrolysis</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D007093" MajorTopicYN="N">Imidazoles</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="N">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D052578" MajorTopicYN="N">Ionic Liquids</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="Y">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D033363" MajorTopicYN="Y">Neutron Diffraction</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D032107" MajorTopicYN="N">Populus</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="Y">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D053838" MajorTopicYN="Y">Scattering, Small Angle</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D014961" MajorTopicYN="Y">X-Ray Diffraction</DescriptorName></MeshHeading></MeshHeadingList><KeywordList Owner="NOTNLM"><Keyword MajorTopicYN="N">Biomass loading</Keyword><Keyword MajorTopicYN="N">Ionic liquid pretreatment</Keyword><Keyword MajorTopicYN="N">Porosity</Keyword><Keyword MajorTopicYN="N">SANS</Keyword><Keyword MajorTopicYN="N">XRD</Keyword></KeywordList></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="received"><Year>2016</Year><Month>12</Month><Day>30</Day></PubMedPubDate><PubMedPubDate PubStatus="revised"><Year>2017</Year><Month>02</Month><Day>03</Day></PubMedPubDate><PubMedPubDate PubStatus="accepted"><Year>2017</Year><Month>02</Month><Day>04</Day></PubMedPubDate><PubMedPubDate PubStatus="pubmed"><Year>2017</Year><Month>2</Month><Day>20</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="medline"><Year>2017</Year><Month>5</Month><Day>10</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="entrez"><Year>2017</Year><Month>2</Month><Day>20</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate></History><PublicationStatus>ppublish</PublicationStatus><ArticleIdList><ArticleId IdType="pubmed">28214697</ArticleId><ArticleId IdType="pii">S0960-8524(17)30121-9</ArticleId><ArticleId IdType="doi">10.1016/j.biortech.2017.02.014</ArticleId></ArticleIdList></PubmedData></pubmed><affiliations><list><country><li>République populaire de Chine</li><li>États-Unis</li></country><region><li>Californie</li><li>Tennessee</li></region><settlement><li>Pékin</li></settlement></list><tree><country name="République populaire de Chine"><noRegion><name sortKey="Yuan, Xueming" sort="Yuan, Xueming" uniqKey="Yuan X" first="Xueming" last="Yuan">Xueming Yuan</name></noRegion><name sortKey="Duan, Yonghao" sort="Duan, Yonghao" uniqKey="Duan Y" first="Yonghao" last="Duan">Yonghao Duan</name></country><country name="États-Unis"><region name="Tennessee"><name sortKey="He, Lilin" sort="He, Lilin" uniqKey="He L" first="Lilin" last="He">Lilin He</name></region><name sortKey="Cheng, Gang" sort="Cheng, Gang" uniqKey="Cheng G" first="Gang" last="Cheng">Gang Cheng</name><name sortKey="Simmons, Blake" sort="Simmons, Blake" uniqKey="Simmons B" first="Blake" last="Simmons">Blake Simmons</name><name sortKey="Singh, Seema" sort="Singh, Seema" uniqKey="Singh S" first="Seema" last="Singh">Seema Singh</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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